RE: [Distillers] 1st still....offset head question
> that the cup under the head (where the needle valve lives) will fillI do something very similar, likewise with 40-50 mL retained there.
> up and overflow into the connector tube and be directed (downhill)
> into the center of the column for reflux. My question is this: in
> order to fill up the cup and begin reflux there will be approximately
> 50 Ml of product in the cup, so when I'm ready to take the foreshots,
> what will be in the cup and how will it affect the removal of the
Its not a problem for me - take out that first 50-80 mL very slowly - 1 drip per second, after 10 minutes equilibrating at full reflux, and it will clean out nicely.